Weak C—H⋯O interactions help to direct the packing, forming sheets lying parallel to (020).In the title compound, C DOI: 10.1107/S2056989015008324/lr2135Isup2.hklStructure factors: contains datablock(s) I. DOI: Click here for additional data file.10.1107/S2056989015008324/lr2135Isup3.cmlSupporting information file. DOI: Click here for additional data file.10.1107/S2056989015008324/lr2135fig1.tif. DOI: The title molecule with labeling scheme and 50% probability ellipsoids.Click here for additional data file.10.1107/S2056989015008324/lr2135fig2.tif . DOI: Packing viewed towards the (101062089CCDC reference:  crystallographic information; 3D view; checkCIF reportAdditional supporting information:


Scientific Reports6: Article number: 20144; 10.1038/srep20144 published online: 02042016; updated: 05202016.In this Article, Figure 3 is incorrect. The correct Figure 3 appears below as


The deprotonated hydroxyl groups of the piperidineethanolate anions bridge CuII cations, forming the tetranuclear complex. All piperidine rings display a chair conformation. In the crystal, there are no significant intermolecular interactions present. The crystal studied was an inversion twin refined with a minor component of 0.18 (5). In the title tetranuclear compound, [Cu DOI: 10.1107/S1600536814009052/xu5784Isup2.hklStructure factors: contains datablock(s) I. DOI: Click here for additional data file.10.1107/S1600536814009052/xu5784Isup3.cdxSupporting information file. DOI: 998731CCDC reference:  crystallographic information; 3D view; checkCIF reportAdditional supporting information:


The line through the I atoms forms an angle of 78.39 (16)° with the normal to the pyridine ring.In the title adduct, C DOI: 10.1107/S2056989015010518/rz5157Isup2.hklStructure factors: contains datablock(s) I. DOI: Click here for additional data file.10.1107/S2056989015010518/rz5157Isup3.cmlSupporting information file. DOI: Click here for additional data file.10.1107/S2056989015010518/rz5157fig1.tif. DOI: The molecular structure of the title compound, with 50% probability displacement ellipsoids for non-H atoms.1404151CCDC reference:  crystallographic information; 3D view; checkCIF reportAdditional supporting information:


AbstractGyponareversa DeLong & Martinson, 1972 has its ovipositor described and illustrated based on the examination of specimens from its type locality. This is the first species of Gypona Germar, 1821 to have the female genitalia detailed description published. Gypona Germar, 1821 (Cicadellidae: Iassinae: Gyponini) includes about 200 described species (Gypona (G.) reversa DeLong & Martinson, 1972 was described based on male holotype  and paratype   . Coelho ae e.g., , we herewww.hadleyweb.pwp.blueyonder.co.uk). Terminalia were stored in a small vial with glycerin pinned below the specimen.The descriptive terminology adopted herein follows mainly The specimen was collected in a fragment of Atlantic Forest inserted on the Universidade Federal de Viçosa (UFV) campus. UFV is located in Viçosa municipality, “Zona da Mata” of Minas Gerais State, southeastern Brazil  and has The specimen examined belongs to Coleção Entomológica José Alfredo Pinheiro Dutra, Departamento de Zoologia (DZRJ), Instituto de Biologia, Universidade Federal do Rio de Janeiro, Rio de Janeiro, Brazil.DeLong & Martinson, 1972Type status:Other material. Occurrence: recordedBy: Luci B. N. Coelho; individualCount: 1; sex: female; lifeStage: adult; Taxon: taxonID: Native; scientificNameID: lsid:zoobank.org:act:8B3CBB30-41F7-4CE3-ADD5-8C00FE4D4D6A; acceptedNameUsage: Gypona reversa DeLong & Martinson, 1972; kingdom: Animalia; phylum: Arthropoda; class: Hexapoda; order: Hemiptera; family: Cicadellidae; genus: Gypona; subgenus: Gypona; specificEpithet: reversa; scientificNameAuthorship: DeLong & Martinson, 1972; Location: continent: South America; country: Brazil; countryCode: BR; stateProvince: Minas Gerais; municipality: Viçosa; locality: Mata da Biologia, Recanto das Cigarras; verbatimElevation: 650 m; verbatimCoordinates: 20°45'31.8"S 42°51'40.5"W; Identification: identifiedBy: Luci B. N. Coelho; dateIdentified: 1993; Event: eventDate: 08/09/1993; Record Level: language: en; institutionCode: DZRJ; collectionCode: Insects; ownerInstitutionCode: Coleção Entomológica Professor José Alfredo Pinheiro Dutra; basisOfRecord: PreservedSpecimenType status:Other material. Occurrence: recordedBy: Luci B. N. Coelho; individualCount: 1; sex: female; lifeStage: adult; Taxon: taxonID: Native; scientificNameID: lsid:zoobank.org:act:8B3CBB30-41F7-4CE3-ADD5-8C00FE4D4D6A; acceptedNameUsage: Gypona reversa DeLong & Martinson, 1973; kingdom: Animalia; phylum: Arthropoda; class: Hexapoda; order: Hemiptera; family: Cicadellidae; genus: Gypona; subgenus: Gypona; specificEpithet: reversa; Location: continent: South America; country: Brazil; countryCode: BR; stateProvince: Minas Gerais; municipality: Viçosa; locality: Mata da Biologia, Recanto das Cigarras; verbatimElevation: 650 m; verbatimCoordinates: 20°45'31.8"S 42°51'40.5"W; Identification: identifiedBy: Luci B. N. Coelho; dateIdentified: 1993; Event: eventDate: 06/28/1993; Record Level: language: en; institutionCode: DZRJ; collectionCode: Insects; ownerInstitutionCode: Coleção Entomológica Professor José Alfredo Pinheiro Dutra; basisOfRecord: PreservedSpecimenGyponareversa DeLong & Martinson, 1972Redescription of femaleLength 7.8 mm. General color green with black and brown spots on pronotum and wings Figs , 2a. Cro2222Forewings translucent, apical region smoky, black spot at the insertion point; brown spot at the apex of each claval vein, inner discal cell with two brown spots, one basal and other apical; irregular brown band from clavus apex to median portion of fifth apical cell; about 3.3 times longer than wide; appendix brown, vestigial.Sternite VII Fig. a, c 2.4 Pygofer, in lateral view, approximately triangular shaped, with apex rounded; scattered macrosetae at posterior margin Fig. d. Ovipos3345545667676739General color green with black and brown spots on pronotum and wings Figs , 2a. Ste2337Brazil  and Mexico  .Wedeliapaludosa DC (Compositae).Specimens were collected in a grove of Atlantic forest, feeding on Studied specimens20°45'31.8"S 42°51'40.5"W , L.B.N. Coelho leg., 1 ♀, 27/vi/1993; 1 ♀, 09/viii/1993 (DZRJ).BRAZIL, Minas Gerais, Viçosa, Universidade Federal de Viçosa, Recanto das Cigarras, Gypona species. Gyponaverticalis Stål, 1864, which is quite shorter than in G.reversa (Fig. 6G.hiata DeLong and Freytag, 1967. Compared with G.hiata, the sternite VII of G.reversa has a more convex lateral margin, and posterior margin with two "teeth" separated by shallow concavity (Fig. 6This is the first published description of the ovipositor valvulae of any ity Fig. a, c; pygity Fig. a, d; venity Fig. b; apicalClinonana Osborn, 1988. Nevertheless, the authors believe that researchers should always make an effort to describe the female genitalia in as much detail as possible, so hopefully in the future it might become a source of useful taxonomic characteristics.According to


The paper:VASOPRESSIN VS TERLIPRESSIN IN TREATMENT OF REFRACTORY SHOCK.Scarpati G., Piazza O.Transl Med UniSa. 2013 Jan 4;5:22–7. has been withdrawn after authors request.The paper:THE NOVEL THERAPEUTHIC TARGETS IN THE TREATMENT OF CHRONIC PAIN.Palomba R., Bonaccia P., Graffi M., Costa F. Transl Med UniSa. 2012 Apr 30;3:57–61. has been withdrawn after authors request.


Scientific Reports6: Article number: 2340310.1038/srep23403; published online: 03212016; updated: 05312016In this Article, Figure 5E and 5F were omitted. The Figure legends are correct. The correct Figure 5 appears below as


Nature Communications6: Article number: 7721 10.1038/ncomms8721 (2015); Published 07132015; Updated 09082015The image in


BMC Ear, Nose and Throat Disorders would like to thank all of our reviewers who have contributed to the journal in Volume 14 (2014).The editors of  Ilona AndersonAustriaMinakshi BhardwajIndiaMarc BraemBelgiumItzhak BrookUSAJosé Cameselle-TeijeiroSpainPeter W. DettmarUKY.P. Peter DiUSAWouter DreschlerNetherlandsCaterina FiniziaSwedenElizabeth FitzpatrickCanadaNoriyuki FujimaJapanKaryn GalvinAustraliaMiguel GoncalvesUKHasantha GunasekeraAustraliaHervé HaasFranceStefan HegemannSwitzerlandSebastian HothGermanyHiroaki IchijoJapanTakao ImaiJapanFikret KasapogluTurkeyTejs KlugDenmarkMasahiro KomoriJapanKenji KondoJapanSeung-Han LeeSouth KoreaDavid J LimUSAFernanda MarianoBrazilElismauro MendoncaBrazilRanko MladinaCroatiaMarkus MoessnerGermanyTsutomu NakashimaJapanGeorge NoussiosGreeceToyoaki OhbuchiJapanBolajoko O. OlusanyaNigeriaFredrik PeterssonSingaporeAntonio SchindlerItalyAiden ShearerUSASivakumaran Theru ArumugamUSAValentino ValentiniItalyFabiana ValeraBrazilKatrien VermeireBelgiumPetros VlastarakosUKChe-Ming WuTaiwanHasan YasanTurkeyBülent YaziciTurkey


An intramolecular C—H⋯Br hydrogen bond forms an S(5) ring motif. In the crystal, weak C—H⋯Br interactions link the molecules into helical chains along the b-axis direction.In the title compound, [SbBr(C DOI: 10.1107/S1600536814020066/is5373Isup2.hklStructure factors: contains datablock(s) I. DOI: Click here for additional data file.10.1107/S1600536814020066/is5373Isup3.cmlSupporting information file. DOI: Click here for additional data file.10.1107/S1600536814020066/is5373fig1.tif. DOI: The molecular structure of the title compound, showing 50% probability displacement ellipsoids. The dashed line indicates the C—H⋯Br hydrogen bond.Click here for additional data file.10.1107/S1600536814020066/is5373fig2.tif. DOI: A crystal packing view of the title compound. Dashed lines indicate hydrogen bonds. H atoms not involved in the hydrogen bonds have been omitted for clarity.1023098CCDC reference:  crystallographic information; 3D view; checkCIF reportAdditional supporting information:


The Li and In atoms are in distorted tetrahedral N2O2 and C2O2 bonding environments, respectively. The Li atom is further chelated by a tmeda group, yielding a spirocyclic structure.The mixed bimetallic title compound, [InLi(CH DOI: 10.1107/S2056989015023476/lh5799Isup2.hklStructure factors: contains datablock(s) I. DOI: Click here for additional data file.10.1107/S2056989015023476/lh5799Isup4.cdxSupporting information file. DOI: Click here for additional data file.10.1107/S2056989015023476/lh5799fig1.tifI . DOI: I), with displacement ellipsoids drawn at the 50% probability level. H atoms have been omitted for clarity.The molecular structure of (1440726CCDC reference:  crystallographic information; 3D view; checkCIF reportAdditional supporting information:


Scientific Reports6: Article number: 23027; 10.1038/srep23027 published online: 03142016; updated: 04292016.In this Article, Figure 4 is a duplication of Figure 6. The correct Figure 4 appears below as


Scientific Reports5: Article number: 1643410.1038/srep16434; published online: 11102015; updated: 01222016This Article contains an error in Fig. 2, where the y-axis ‘Herbage mass ln + 1(t/ha)’ was incorrectly given as ‘Herbage mass ln + 1(kg/ha)’. The correct Fig. 2 appears below as


The deprotonated ligands act as N,S-donors, forming five-membered metalla-rings. The NiII atom is four-coordinated in a slightly distorted square-planar environment. In the crystal, the discrete complex molecules are linked by weak N—H⋯O hydrogen bonds, generating chains along [110]. The chains are further connected via weak O—H⋯N interactions into a layered network extending parallel to (001).In the title compound, [Ni(C DOI: 10.1107/S1600536814009027/lr2126Isup2.hklStructure factors: contains datablock(s) I. DOI: 998671CCDC reference:  crystallographic information; 3D view; checkCIF reportAdditional supporting information:


Nature Communications 6: Article number: 8191 doi: 10.1038/ncomms9191 (2015); Published 09042015; Updated 10132015An incorrect version of the Supplementary Figure 1-4, Supplementary Table 1, Supplementary Methods and Supplementary References


Nature Communications6: Article number: 10116 10.1038/ncomms10116 (2015); Published: 12022015; Updated: 04202016In Fig. 6f of this article, the histogram label ‘Lsd1' should read ‘IAP'. The correct version of Fig. 6 appears below.Figure 6


AbstractIdiopyga Savchenko, 1987 is a northern hemisphere group of short-palped crane flies . In the current article we describe a new species, Dicranomyia (I.) boreobaltica Salmela sp.n., and redescribe the male and female post-abdomen of a closely related species, D. (I.) intricata Alexander. A standard DNA barcoding fragment of 5′ region of the cytochrome c oxidase I (COI) gene of the new species is presented, whilst the K2P minimum distances between the new species and 10 other species of the subgenus were found to range from 5.1 to 15.7 % (mean 11.2 %). Phylogenetic analyses (parsimony and maximum likelihood) based on COI sequences support the identity of the new species and its close relationship with D. (I.) intricata and D. (I.) esbeni (Nielsen). The new species is known from the northern Baltic area of Finland. The new species has been mostly collected from Baltic coastal meadows but an additional relict population is known from a calcareous rich fen that was estimated to have been at sea level circa 600-700 years ago. Dicranomyia (I.) intricata (syn. D.suecica Nielsen) is a Holarctic species, occurring in the north boreal and subarctic vegetation zones in Fennoscandia.The subgenus  D. (I.) magnicauda Lundström, D. (I.) murina (Zetterstedt) and D. (I.) ponojensis Lundström. A few species, or taxa that are recognised as subspecies, may have very restricted ranges (e.g. D. (I.) melleicaudastenoptera Savchenko [D. (I.) lulensis (Tjeder) [D. (I.) esbeni (Nielsen) [Dicranomyia (Idiopyga) species are characterised by a complicated structure of male hypopygium, having appendages on their ventral gonostylus and gonocoxite. The female cerci are very short in species such as D. (I.) intricata Alexander and D. (I.) lulensis whereas a normal length  in e.g. D. (I.) halterella Edwards and D. (I.) ponojensis. Species of the subgenus occur around temperate and subarctic wetlands (Tjeder) ) or disjNielsen) ). Dicrannds e.g. , and somnds e.g. .Dicranomyia (I.) intricata was reported from Finland by Nieminen (http://www.finbol.org/eng/ENG_finbol.html), an abnormal intraspecific divergence was noted among the sequenced D. (I.) intricata specimens. Followed up by morphological examinations of voucher specimens, it was obvious that instead of one species there were two, distinguishable on both molecular and morphological basis (D. (I.) intricata, D.suecica (Nielsen)) allowed us to associate our morphospecies to taxonomic species. In the current article we describe a new Dicranomyia species from Finland and redescribe male and female post-abdomen of D. (I.) intricata. The new species is hitherto known from the northern Baltic area whereas D. (I.) intricata has a Holarctic range. To summarize, the approach we use is integrative  was sequenced from a total of 22 Dicranomyia specimens and one Metalimnobia specimen. Legs or 2–3 abdominal segments of the specimens were placed in 96% ethanol in a 96-well lysis microplate and dispatched to the Canadian Centre for DNA Barcoding, Biodiversity Institute of Ontario where DNA was extracted and sequenced using standard protocols and primers (D. (I.) esbeni for which the last 51 basepairs were missing due to sequencing problems. The new sequences are deposited in GenBank under accession numbers KP064165-KP064187  analysis in TNT  version 1.1 . Nodal sMaximum likelihood approachMaximum likelihood analysis was conducted with RAxML ver. 8.0.22  in the CSalmelasp. n.urn:lsid:zoobank.org:act:5537A033-CC12-41C0-869C-F603D8775005Type status:Holotype. Occurrence: catalogNumber: JES-20120094; recordedBy: T. Nieminen; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: boreobaltica; scientificNameAuthorship: Salmela; Location: country: Finland; stateProvince: Ostrobothnia borealis pars ouluensis; verbatimLocality: Oulunsalo, Papinkari; verbatimLatitude: 64.9060; verbatimLongitude: 25.3764; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: Malaise trap; eventDate: 2005-8-11/10-8; habitat: Baltic coastal meadow; Record Level: institutionCode: ZMUTType status:Paratype. Occurrence: recordedBy: T. Nieminen; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: boreobaltica; scientificNameAuthorship: Salmela; Location: country: Finland; stateProvince: Ostrobothnia borealis pars ouluensis; verbatimLocality: Hailuoto, Pökönnokka; verbatimLatitude: 65.0790; verbatimLongitude: 24.8883; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: Malaise trap; eventDate: 2005-8-11/10-8; habitat: Baltic coastal meadow; Record Level: institutionCode: JSOType status:Paratype. Occurrence: recordedBy: T. Nieminen; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: boreobaltica; scientificNameAuthorship: Salmela; Location: country: Finland; stateProvince: Ostrobothnia borealis pars ouluensis; verbatimLocality: Hailuoto, Pökönnokka; verbatimLatitude: 65.0790; verbatimLongitude: 24.8883; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: Malaise trap; eventDate: 2005-8-11/10-8; habitat: Baltic coastal meadow; Record Level: institutionCode: ZMUTType status:Paratype. Occurrence: catalogNumber: DIPT-JS-2014-0248; recordedBy: J. Salmela; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: boreobaltica; scientificNameAuthorship: Salmela; Location: country: Finland; stateProvince: Ostrobothnia borealis pars borealis; verbatimLocality: Tornio, Isonkummunjänkä Mire Conservation Area, Kusiaiskorpi; verbatimLatitude: 65.8880; verbatimLongitude: 24.4792; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: Malaise trap; eventDate: 2013-8-1/9-26; habitat: Rich fen, rusty spring; Record Level: institutionCode: JESType status:Paratype. Occurrence: catalogNumber: DIPT-JS-2014-0251; recordedBy: J. Salmela; individualCount: 1; sex: female; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: boreobaltica; scientificNameAuthorship: Salmela; Location: country: Finland; stateProvince: Ostrobothnia borealis pars borealis; verbatimLocality: Tornio, Isonkummunjänkä Mire Conservation Area, Kusiaiskorpi; verbatimLatitude: 65.8880; verbatimLongitude: 24.4792; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: Malaise trap; eventDate: 2013-8-1/9-26; habitat: Rich fen, rusty spring; Record Level: institutionCode: JESType status:Paratype. Occurrence: recordedBy: J. Salmela; individualCount: 1; sex: female; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: boreobaltica; scientificNameAuthorship: Salmela; Location: country: Finland; stateProvince: Ostrobothnia borealis pars borealis; verbatimLocality: Tornio, Isonkummunjänkä Mire Conservation Area, Kusiaiskorpi; verbatimLatitude: 65.8880; verbatimLongitude: 24.4792; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: Malaise trap; eventDate: 2013-8-1/9-26; habitat: Rich fen, rusty spring; Record Level: institutionCode: ZMUTType status:Other material. Occurrence: catalogNumber: DIPT-JS-2014-0114; recordedBy: J. Salmela; individualCount: 7; sex: 4 females, 3 males; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: boreobaltica; scientificNameAuthorship: Salmela; Location: country: Finland; stateProvince: Ostrobothnia borealis pars borealis; verbatimLocality: Tornio, Isonkummunjänkä Mire Conservation Area, Kusiaiskorpi; verbatimLatitude: 65.8880; verbatimLongitude: 24.4792; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: Malaise trap; eventDate: 2013-8-1/9-26; habitat: Rich fen, rusty spring; Record Level: institutionCode: JESDicranomyia (Idiopyga) intricataDicranomyia (Idiopyga) cf.intricataHead. Vertex dark brown, with short black setae. Rostrum light brown with a few short dark setae. Palpus 5-segmented; first palpomere very short, globular, 1.5 times wider than long; other palpomeres elongated, p2 length 140 µm, p3 100 µm, p4 100 µm and p5 120 µm. First palpomere with a long ventral seta, approximately 2 times longer than width of palpomere. Second and third palpomeres with 5 setae, arranged in the apical half of segments. Fourth palpomere bearing ca. 12 setae and p5 with 13-15 setae, most of these on the apices of the segments. Antennae 14-segmented, dark brown, segments bearing black setae mostly exceeding width of respective segment; setae straight on scape (ca. 10 setae) and pecidel (ca. 15 setae), straight or curved on flagellomeres (ca. 5 setae on each flagellomere). Scape cylindrical, length 200 µm, width 75 µm, pedicel wider apically than basally, length 115 µm, width 75 µm. Flagellomeres oval, longer than wide; f1 length 120 µm, width 65 µm, f2 length 8 µm, width 5 µm, f10 length 110 µm, width 40 µm. Thorax mainly dark brown. Prescutum dark brown, only small yellowish spots on hind lateral corners. Scutum dark brown with longitudinal yellow median line and yellow lateral spots near wing base. Mediotergite and anepisternum dark brown, mediotergite sometimes with narrow yellowish anterior margin. Laterotergite and anepimeron yellowish brown. Katepisternum bicolored: anterior half dark brown, posterior half yellowish brown. Fore coxa brown, mid and hind coxae yellowish brown. Femorae light brown or brown, tibiae and tarsi dark brown. Length of fore femora 4500 µm, tibia 5250 µm, t1 3500 µm, t2 1100 µm, t3 875 µm, t4 300 µm, t5 175 µm, claw 130 µm. Length of mid femora 5575 µm, tibia 5625 µm, t1 3200 µm, t2 1150 µm, t3 625 µm, t4 275 µm, t5 175 µm, claw 130 µm. Length of hind femora 5600 µm, tibia 5750 µm, t1 3050 µm, t2 1150, t3 650 µm, t4 275 µm, t5 178 µm, claw 130 µm. Halter grayish-brown. Wing clear, veins light brown - brown, pterostigma brown  intricata. Ventrobasal lobe of ventral gonostylus sinuous, apex oval. Inner appendage of gonocoxite apically rounded. Rostral prolongantion of ventral apically rather narrow and subrostral prolongation simple, not bilobed, bearing dark stout spines. Female infra-anal plate with strong caudal peak.Brownish, small species, very close to borealis, Latin)= north, baltica (Latin)= referring to the Baltic Sea. The species is so far known from the northern Baltic area. The species name is deemed to be a latinized adjective in nominative singular.Boreo  intricata). These coastal meadows are produced by a phenomenon called land uplift, that is, the rebound of earth's crust after the retreating of the ice sheet; in the Bothnian Bay the rate of land uplift is about 8 mm/year (D. (I.) boreobaltica Salmela sp.n. is a recent relict species in the fen. It should be noted that some plants typical for the Baltic shores or brackish water have isolated populations on calcareous ponds or mires far from coastal areas  boreobaltica Salmela sp.n. was absent from the samples. This and other negative records (i.e. absence) from >500 Malaise trapping sites in Finnish wetlands  and insect  species in the Baltic coastal areas (D. (I.) boreobaltica Salmela sp.n. could either be i) a recently evolved allopatric species that survived Pleistocene glaciations and is currently only present in the Baltic area or ii) a disjunct species having populations in other  areas.Due to its apparent rarity, that is, small area of occupancy and extent of occurrence, the species could most likely be assessed as a threatened species according to IUCN criteria. Habitats of this species are highly endangered, usually small and isolated. There are a total of ca. 4200 ha of Baltic coastal meadows along the Finnish coast, and all such habitat types are red-listed . Also spal areas . Hence, D. (I.) intricata. As already stated in the title of this article, the new species is cryptic, meaning that it is hard to distinguish from its sister species by morphological characters. Strictly speaking, cryptic species may mean taxa that are morphologically indisguishable  boreobaltica Salmela sp.n. and D. (I.) intricata are not separated by a distinct barrier, they have non-overlapping ranges perhaps because of biogeographic factors driven by climate  boreobaltica Salmela sp.n. and D. (I.) intricata are practically identical. The most important differences in male and female post-abdomen between the species are summarized in Table D. (Idiopyga) species, the new species is quite close to D. (I.) esbeni. Besides other details, the ventrobasal lobe of gonocoxite in D. (I.) esbeni is sinuous (see D. (I.) boreobaltica Salmela sp.n. Dicranomyia (I.) melleicauda complicata de Meijere is also quite close to the new species, but has rather stout iagx and apically wide lvg  sequence of Dicranomyia (I.) boreobaltica Salmela sp.n. BOLD Sample ID JES-20120094, holotype specimen:Standard 5′ region (658 bp) of the cytochrome TACCTTATACTTTATTTTTGGAGCTTGAGCAGGAATAGTGGGAACTTCATTAAGTATTATTATTCGAGCAGAATTAGGACACCCAGGTGCATTAATTGGAGACGACCAGATTTATAATGTGGTAGTTACTGCCCATGCTTTTATTATAATTTTCTTTATAGTTATACCAATTATAATTGGAGGATTCGGTAATTGATTAGTTCCTTTAATATTAGGAGCCCCAGATATAGCTTTCCCTCGAATAAATAATATAAGTTTTTGAATACTTCCCCCTTCTTTAACTTTATTATTAGCTAGAAGCATAGTTGAAAACGGGGCAGGAACTGGCTGAACAGTATACCCTCCCCTTTCTTCTGGAATTGCCCATTCAGGGGCTTCTGTAGATTTAGCTATTTTTTCTCTTCACCTAGCAGGTATTTCTTCTATTTTAGGAGCTGTTAATTTTATTACAACTGTTATTAATATACGTTCAGCAGGAATTTCATTTGATCGAATACCATTATTTGTTTGATCAGTAGTAATTACTGCTATTTTATTGCTTTTATCACTTCCTGTTTTAGCCGGAGCTATTACAATATTATTAACAGATCGAAACTTAAATACTTCATTTTTTGATCCCGCAGGTGGAGGAGACCCTATTTTATATCAGCATTTATTTD. (I.) intricata (K2P distance 5.13 %), D. (I.) esbeni (7.16 %) and D. (I.) magnicauda (9.51 %); other distances within examined D. (Idiopyga) species range between 10.76 and 15.70 %.Based on K2P  distanceAlexander, 1927Type status:Holotype. Occurrence: recordedBy: O. Bryant; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Canada; stateProvince: Alberta; verbatimLocality: Lesser Slave Lake; verbatimLatitude: 55.35; verbatimLongitude: -115.09; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: eventDate: 1924-8-1; Record Level: institutionCode: USNMType status:Paratype. Occurrence: recordedBy: O. Bryant; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Canada; stateProvince: Alberta; verbatimLocality: Lesser Slave Lake, Grizzly mt.; minimumElevationInMeters: 914; Event: eventDate: 1924-8-15; Record Level: institutionCode: USNMType status:Holotype. Occurrence: catalogNumber: 855; recordedBy: H. Frantz; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: suecica; scientificNameAuthorship: Nielsen; Location: country: Sweden; stateProvince: Abisko; verbatimLatitude: 68.35; verbatimLongitude: 18.79; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: eventDate: unknown; Record Level: institutionCode: ZMUCType status:Other material. Occurrence: recordedBy: P.T. Bruggemann; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Canada; stateProvince: Yukon; verbatimLocality: Dawson; minimumElevationInMeters: 335; Event: eventDate: 1949-8-6; Record Level: institutionCode: USNMType status:Other material. Occurrence: recordedBy: W.W. Moss; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Canada; stateProvince: British Columbia; verbatimLocality: Telegraph Creek; minimumElevationInMeters: 335; Event: eventDate: 1960-8-28; Record Level: institutionCode: USNMType status:Other material. Occurrence: recordedBy: W.W. Moss; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Canada; stateProvince: British Columbia; verbatimLocality: Telegraph Creek, Sawmill Lake; Event: eventDate: 1960-8-18; Record Level: institutionCode: USNMType status:Other material. Occurrence: recordedBy: O. Bryant; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Canada; stateProvince: Northwest Territories; verbatimLocality: Aklavik; Event: eventDate: 1931-8-27; Record Level: institutionCode: USNMType status:Other material. Occurrence: catalogNumber: JES-20120082; recordedBy: J. Salmela; individualCount: 1; sex: female; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Finland; stateProvince: Lapponia kemensis pars occidentalis; verbatimLocality: Kittilä, Mustaoja-Nunaravuoma Mire Conservation Area, Mustaoja W; verbatimLatitude: 67.6390; verbatimLongitude: 25.4277; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: sweep net; eventDate: 2009-8-19; habitat: rich flark fen; Record Level: institutionCode: ZMUTType status:Other material. Occurrence: catalogNumber: DIPT-JS-2014-0336; recordedBy: J. Salmela; individualCount: 32; sex: 29 male, 3 female; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Finland; stateProvince: Lapponia enontekiensis; verbatimLocality: Enontekiö, Tarvantovaara Wilderness Area, Tomuttirova W; verbatimLatitude: 68.6369; verbatimLongitude: 22.5381; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: sweep net; eventDate: 2009-8-26; habitat: swampy flark fen; Record Level: institutionCode: JESType status:Other material. Occurrence: catalogNumber: JES-20110082; recordedBy: J. Salmela; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Finland; stateProvince: Lapponia enontekiensis; verbatimLocality: Enontekiö, Tarvantovaara Wilderness Area, Tomuttirova W; verbatimLatitude: 68.6369; verbatimLongitude: 22.5381; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: sweep net; eventDate: 2009-8-26; habitat: swampy flark fen; Record Level: institutionCode: ZMUTType status:Other material. Occurrence: catalogNumber: DIPT-JS-2014-0337; recordedBy: J. Salmela; individualCount: 10; sex: 5 male, 5 female; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Finland; stateProvince: Lapponia enontekiensis; verbatimLocality: Enontekiö, Tarvantovaara Wilderness Area, Tomuttirova N; verbatimLatitude: 68.6391; verbatimLongitude: 22.5518; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: sweep net; eventDate: 2009-8-26; habitat: intermediate rich flark fen; Record Level: institutionCode: JESType status:Other material. Occurrence: catalogNumber: DIPT-JS-2014-0182; recordedBy: J. Salmela; individualCount: 1; sex: male; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Finland; stateProvince: Lapponia kemensis pars orientalis; verbatimLocality: Sodankylä, Pomokaira-Tenniöaapa Mire Conservation Area, Syväkuru; verbatimLatitude: 67.8718; verbatimLongitude: 26.2126; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: Malaise trap; eventDate: 2013-8-15/9-19; habitat: spring fen; Record Level: institutionCode: JESType status:Other material. Occurrence: catalogNumber: DIPT-JS-2014-0338; recordedBy: J. Salmela; individualCount: 4; sex: 1 male, 3 female; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Finland; stateProvince: Ostrobothnia borealis pars borealis; verbatimLocality: Kemijärvi, Salmiaavanhete; verbatimLatitude: 66.9929; verbatimLongitude: 27.0578; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: sweep net; eventDate: 2009-8-15; habitat: rich flark fen; Record Level: institutionCode: JESType status:Other material. Occurrence: catalogNumber: DIPT-JS-2014-0340; recordedBy: J. Salmela; individualCount: 1; sex: 1 female; Taxon: genus: Dicranomyia; subgenus: Idiopyga; specificEpithet: intricata; scientificNameAuthorship: Alexander; Location: country: Finland; stateProvince: Lapponia inariensis; verbatimLocality: Inari, Kaunispää; verbatimLatitude: 68.4461; verbatimLongitude: 27.4351; verbatimCoordinateSystem: decimal degrees; verbatimSRS: WGS84; Event: samplingProtocol: sweep net; eventDate: 2013-8-16; habitat: alpine wetland; Record Level: institutionCode: JESDicranomyiaintricataLimonia (Dicranomyia) suecicaLimonia (Dicranomyia) suecicaDicranomyia (Idiopyga) intricataD. (I.) intricata  intricata by D.suecica is lost , but based on Tjeder's detailed illustrations this nomenclature can be verified. Alexander's original description is good, and there is no need to thoroughly re-describe this species. However, male and female genitalia are illustrated here and diagnostic characters are discussed under D. (I.) boreobaltica Salmela sp.n.The holotype specimen of ata Fig. a is in gata Fig. , fig. 1 ata Fig. b. The hoy Tjeder  and the D. (I.) boreobaltica Salmela sp.n., see Fig. 101010Male hypopygium. 9th tergite and proctiger as in Fig. 10Female postabdomen. Cerci and hypogynial valves, see Fig. D. (I.) intricata is known from the north boreal ecoregion, both from the zone of coniferous forests and from the subarctic fell area in the northernmost part of the country , Sweden  intricata (Sphagnum mosses (http://en.wikipedia.org/wiki/Muskeg). Most of the Finnish sampling sites are aapamires, that is, minerotrophic fens with wet, usually moss covered, flarks (hollows) and drier hummock-level strings. Most of the sites are intermediate rich or rich fens, characterised by brown mosses . The species was especially abundant on two closely lying intermediate rich, Sphagnum dominated aapamires in Enontekiö, NW Finnish Lapland, but single specimens were also caught along a spring and a headwater stream  intricata is red-listed in Finland  intricata is absent from the northern Baltic coastal area and is replaced there by a sibling species (D. (I.) boreobaltica sp.n. Salmela). Thus the range ("extent of occurrence") of D. (I.) intricata is actually smaller that was thought in the 2010 assessment. However, the species is not extremely rare and there are most likely hundreds of square kilometres of suitable breeding sites for the species in Finnish Lapland. Nevertheless, the species may be jeopardized by climate change and it may also be used as an indicator of pristine boreal mires.land NT, . At the Dicranomyia (I.) boreobaltica Salmela sp.n.See c oxidase I (COI) gene of Dicranomyia (I.) intricata :Standard 5′ region (658 bp) of the cytochrome TACCTTATACTTTATTTTTGGAGCTTGAGCAGGAATAGTAGGAACTTCACTAAGTATTATTATTCGAGCAGAATTAGGACACCCAGGAGCATTAATTGGAGATGACCAAATTTATAATGTAGTAGTTACTGCCCATGCTTTTATTATAATTTTTTTTATAGTTATACCAATTATAATTGGTGGATTCGGTAATTGATTAGTTCCTTTAATATTAGGAGCCCCAGATATAGCTTTCCCTCGAATAAATAATATAAGTTTTTGAATACTTCCCCCTTCTTTAACCTTATTATTAGCTAGAAGTATAGTTGAAAACGGGGCAGGAACTGGTTGAACAGTTTACCCTCCCCTTTCTTCTGGAATTGCTCATTCAGGAGCTTCTGTAGACTTAGCTATTTTTTCTCTTCATTTAGCAGGTATTTCTTCTATTTTAGGAGCTGTTAACTTTATTACAACTGTTATTAATATACGTTCAGCAGGAATTTCATTCGACCGAATACCATTATTTGTTTGATCAGTAGTAATTACTGCTATTCTATTACTCTTATCACTCCCTGTTTTAGCTGGAGCTATTACAATATTATTAACAGATCGAAACTTAAACACTTCATTTTTTGACCCTGCAGGTGGAGGAGATCCTATTTTATACCAACACTTATTTL = -3501.956818) in Fig. 13D. (I.) boreobaltica Salmela sp.n. as sister to D. (I.) intricata and these two species grouping together with D. (I.) esbeni. Nodal supports in both results are good giving strong indications that D. (I.) boreobaltica Salmela sp.n. forms its own group being in a sister group relationship with D. (I.) intricata. There are altogether 31 bases in COI that differ between D. (I.) boreobaltica Salmela sp.n. and D. (I.) intricata, resulting in 4.7 % difference between these species. Although nodal supports in the deeper, evolutionary older nodes are low, separate species are clearly distinct.The phylogenetic tree (length 622 steps) resulting from the parsimony analysis is shown in Fig. 13Supplementary material 1Diptera, Limoniidae), USNMDicranomyia (I.) intricata Alexander, 1927 (Data type: imagesDicranomyia (I.) intricata Alexander, males, permanently slide-mounted by C.P. Alexander, deposited in USNM . Digital photos of the slides.Brief description: Non-type material of File: oo_33643.pdfJukka SalmelaSupplementary material 2COI sequences of Dicranomyia (Idiopyga) species and three out-group speciesData type: GenomicBrief description: COI 5' standard DNA barcoding fragmentFile: oo_33852.txtJukka Salmela


The incidence of oropharyngeal cancer is increasing in the developed world. This has led to a large rise in research activity and clinical trials in this area, yet there is no consensus on which outcomes should be measured. As a result, the outcomes measured often differ between trials of comparable interventions, making the combination or comparison of results between trials impossible. Outcomes may also be ‘cherry-picked’, such that favourable results are reported, and less favourable results withheld. The development of a minimum outcome reporting standard, known as a core outcome set, goes some way to addressing these problems. Core outcome sets are ideally developed using a patient-centred approach so that the outcomes measured are relevant to patients and clinical practice. Core outcome sets drive up the quality and relevance of research by ensuring that the right outcomes are consistently measured and reported in trials in specific areas of health or healthcare.This is a mixed methods study involving three phases to develop a core outcome set for oropharyngeal cancer clinical trials. Firstly, a systematic review will establish which outcomes are measured in published oropharyngeal cancer randomised controlled trials (RCTs). Secondly, qualitative interviews with patients and carers in the UK and the USA will aim to establish which outcomes are important to these stakeholders. Data from these first two stages will be used to develop a comprehensive list of outcomes to be considered for inclusion in the core outcome set. In the third stage, patients and clinicians will participate in an iterative consensus exercise known as a Delphi study to refine the contents of the core outcome set. This protocol lays out the methodology to be implemented in the CONSENSUS study.A core outcome set defines a minimum outcome reporting standard for clinical trials in a particular area of health or healthcare. Its consistent implementation in oropharyngeal cancer clinical trials will improve the quality and relevance of research.13823 (17 January 2013).This study is registered at the National Institute for Health Research (NIHR) Clinical Research Network (CRN) portfolio, ID  Around 1,500 cases of oropharyngeal squamous cell carcinoma (OPSCC) are diagnosed in the UK every year 2. (“Head and Neck Neoplasms”[Mesh:NoExp])3. “Otorhinolaryngologic Neoplasms”[Mesh:NoExp]4. “Pharyngeal Neoplasms”[Mesh:NoExp]5. “Neoplasms”[Mesh]6. 9. (#5 OR #6)10. “Oropharynx”[Mesh]11. 12. (#10 OR #11)13. (#9 AND #12)14. (HNSCC ORSCCHN OR OP-SCC OR OPSCC)15. (#1 OR #2 OR #3 OR #4 OR #13 OR #14)16. ) OR ) OR ) OR  OR  OR  OR  OR  OR  OR  OR  OR (“Multicenter Study”[Publication Type]) OR (“Multicenter Studies as Topic”[Mesh]) OR (“Random Allocation”[Mesh]) OR (“Double-Blind Method”[Mesh]) OR (“Single-Blind Method”[Mesh]) OR (“Cross-Over Studies”[Mesh]) OR (“Placebos”[Mesh]) OR ) OR (blind[tiab] OR blinding[tiab] OR blinded[tiab] OR mask[tiab] OR masking[tiab] OR masked[tiab] OR placebo[tiab] OR placebos[tiab] OR rct[tiab] OR random[tiab] OR randomised[tiab] OR randomized[tiab] OR randomly[tiab] OR randomisation[tiab] OR randomization[tiab]) OR  OR (divided[tiab] AND (group[tiab] OR groups[tiab])) OR (crossover[tiab]) OR (“cross over”[tiab]) OR (multicentre[tiab] OR multicentred[tiab] OR multicentric[tiab]) OR (versus[ti] OR vs[ti]) OR (“treatment arm”[tiab]) OR (“phase III”[tiab] OR “phase three”[tiab] OR “phase 3”[tiab]) OR (“latin square”[tiab]) NOT  NOT  AND (“Humans”[Mesh])))))17. (#15 AND #16)18. ““Cochrane Database Syst Rev”“[Journal]19. 20. (#19 OR #18)21. (#17 NOT #20)Cochrane Central Register of Controlled Trials (CENTRAL): 1 January 2003 to 14 May 20131. MeSH descriptor: [Oropharyngeal Neoplasms] explode all trees2. MeSH descriptor: [Head and Neck Neoplasms] this term only3. MeSH descriptor: [Pharyngeal Neoplasms] this term only4. MeSH descriptor: [Otorhinolaryngologic Neoplasms] this term only5. MeSH descriptor: [Neoplasms] explode all trees6. cancer* OR carcinoma* OR neoplas* OR tumor* OR tumour* OR malignan* OR SCC7. #5 OR #68. MeSH descriptor: [Oropharynx] explode all trees9. oropharyn* OR mesopharyn* OR tonsil* OR “head and neck” OR “head neck” OR “head-neck” OR “head-and-neck” OR pharyn* OR “tongue base” OR “soft palate”10. #8 OR #911. #7 AND #1012. HNSCC OR SCCHN OR OP-SCC OR OPSCC13. #1 OR #2 OR #3 OR #4 OR #11 OR #12Embase: 1 January 2003 to 14 May 20131. Exp Oropharynx tumor/2. Pharynx cancer/3. Neoplasm/4. .tw.5. #3 OR #46. exp OROPHARYNX/OR exp OROPHARYNX CANCER/OR exp OROPHARYNX CARCINOMA/7. .tw.8. #6 OR #79. #5 AND #810. (HNSCC OR SCCHN OR OP-SCC OR OPSCC).tw.11. #1 OR #2 OR #9 OR #1012. .mp. OR crossover*.tw. 13. (cross adj over*).tw.14. (cross adj over*).tw.15. ((blind* OR mask*) and (single OR double OR triple OR treble)).tw.16. (treatment adj arm*).tw.17. (control* adj group*).tw.18. (phase adj III).mp. OR three.tw. 19. (versus OR vs).tw.20. rct.tw.21. CROSSOVER PROCEDURE/22. DOUBLE BLIND PROCEDURE/23. SINGLE BLIND PROCEDURE/24. RANDOMIZATION/25. PLACEBO/26. exp CLINICAL TRIAL/27. PARALLEL DESIGN/28. LATIN SQUARE DESIGN/29. #12 OR #13 OR #14 OR #15 OR #16 OR #17 OR #18 OR #19 OR #20 OR #21 OR #22 OR #23 OR #24 OR #25 OR #26 OR #27 OR #2830. #11 AND #2931. limit #30 to human32. “systematic review”.tw.33. #31 NOT #32CENTRAL: Cochrane Central Register of Controlled Trials; CNS: Clinical nurse specialist; COMET: Core Outcome Measures in Effectiveness Trials; CRT: Chemoradiotherapy; HPV: Human papillomavirus; HPV-16: Human papillomavirus type 16; HTA: Health Technology Assessment; ICF: International Classification of Functioning, Disability and Health; NHS: National Health Service; NIHR: National Institute for Health Research; OMERACT: Outcome Measures in Rheumatology; OPSCC: Oropharyngeal squamous cell carcinoma; PI: Principal investigator; PRO: Patient-reported outcome; RA: Rheumatoid arthritis; RCT: Randomised controlled trial; RT: Radiotherapy; SCCHN: Squamous cell carcinoma of the head and neck; SLT: Speech and language therapist.The authors declare that they have no competing interests.AW conceived and designed the study, and wrote the manuscript. CTS conceived and designed the study, and provided critical revision of the manuscript. BY conceived and designed the study, and provided critical revision of the manuscript. TMJ conceived and designed the study, and provided critical revision of the manuscript. All authors read and approved the final manuscript.


Scientific Reports6: Article number: 2977910.1038/srep29779; published online: 07152016; updated: 08162016This Article contains typographical errors in Table 1. In the column ‘Slip (twinning) system’, the seventh {332} <113> twin value “(3


The correct name is: Petr Stastny. The correct citation is: Petr M, Stastny P, Pecha O, Šteffl M, Šeda O, Kohlíková E (2014) PPARA Intron Polymorphism Associated with Power Performance in 30-s Anaerobic Wingate Test. PLoS ONE 9(9): e107171. doi:


The second half is gererated by inversion symmetry. The crystal structure has a layered arrangement built from distorted edge-sharing LiO3(OH)2 tetrahedra parallel to (100), with naphthalenedicarboxylate bridging the LiO3(OH)2 layers along the [100] direction. Hydrogen bonding between the water molecule and adjacent carboxylate groups consolidates the packing.The title compound, [Li DOI: 10.1107/S1600536814013130/pj2011Isup2.hklStructure factors: contains datablock(s) I. DOI: Click here for additional data file.10.1107/S1600536814013130/pj2011Isup3.molSupporting information file. DOI: 1006973CCDC reference:  crystallographic information; 3D view; checkCIF reportAdditional supporting information:


In the crystal, C—H⋯O hydrogen-bond interactions link the molecules into chains running parallel to the b axis.The molecule of the commercially available title compound, C DOI: 10.1107/S2056989015008816/rz5158Isup2.hklStructure factors: contains datablock(s) I. DOI: Click here for additional data file.10.1107/S2056989015008816/rz5158Isup3.cmlSupporting information file. DOI: Click here for additional data file.10.1107/S2056989015008816/rz5158fig1.tif. DOI: The molecular structure of title compound with displacement ellipsoids drawn at the 30% probability level.Click here for additional data file.10.1107/S2056989015008816/rz5158fig2.tifb via . DOI: b axis via C—H⋯O hydrogen bonds (dashed lines). H atoms not involved in hydrogen bonding are omitted.Crystal packing of the title compound, showing the formation of chains parallel to the 1063415CCDC reference:  crystallographic information; 3D view; checkCIF reportAdditional supporting information: